Design and construction of a sampling system that can collect PM10, PM2.5 and PM1 samples simultaneously from atmosphere

Download
2019
Ateş, Ömer
In this study, a particulate matter (PM) sampling system that can collect PM10 (particulate matter with diameter of less than 10 μm), PM2.5 and PM1 samples simultaneously with a single pump on separate filters was constructed and validated. The sampler consisted of a F&J Specialty DF-1E carbon vane vacuum pump, with a flowrate of 115 L/min, and 3 channels connected to the pump through a manifold. Each channel had a cyclone, a filter holder of 47 mm diameter, a micro-orifice (critical orifice) for velocity control and a flowmeter. Diameter of the particles were controlled by the cyclones. The particles passing through the cyclones was collected at the filters. The sampler was first constructed with MFCs, then MFCs were replaced with critical orifices. Afterwards, components were placed into the permanent shelter and data logger system was installed and flow rate stability tests were carried out using Nuclepore and Teflon filters. Teflon filters were selected for better stability. Validation was carried out through parallel sampling of the new sampler against 1 SFU, 2 Hi-vol samplers and 1 Grimm EDM164 laser spectrometer for 24 days. Average concentrations were found for PM10, PM2.5 and PM1 as 25 ± 10, 13 ± 4.4 and 7.6 ± 2.9 µg m-3 respectively, which were in a good agreement with other samplers. The sampler constructed in this study is not currently available in the market and the final configuration cost around 57,000 ₺ (~$15,700) which is less than half of dichotomous sampler or 3 pcs. of single channel samplers that can fulfill the same sampling task.

Suggestions

Investigation of passive sampling of no2 and o3 in ambient air and determination of the effects of meteorological parameters to the uptake rate
Bayındır, Elif; Tuncel, Semra G.; Department of Chemistry (2008)
In this study NO2 and O3 gases which are the secondary pollutants in ambient air were sampled with designed passive tubes. The collected samples were extracted for UV-VIS spectrometric analysis. NO2 gases were converted to NO2- ions by extracting with water and then this solution was colored with Saltzman reagent (5:1 sulfanilamide and N-(1 naphthly)-ethlyene-diamine dihydrochloride). Then the absorbance of the solution was measured at 537 nm. O3 was extracted with 3-metyl-2-benzothiazolinone hydrozone hydr...
An evaluation of potential sampling locations in a reservoir with emphasis on conserved spatial correlation structure
YENİLMEZ, Firdes; Duzgun, Sebnem; Aksoy, Ayşegül (2015-01-01)
In this study, kernel density estimation (KDE) was coupled with ordinary two-dimensional kriging (OK) to reduce the number of sampling locations in measurement and kriging of dissolved oxygen (DO) concentrations in Porsuk Dam Reservoir (PDR). Conservation of the spatial correlation structure in the DO distribution was a target. KDE was used as a tool to aid in identification of the sampling locations that would be removed from the sampling network in order to decrease the total number of samples. Accordingl...
Analysis of the Raman intensities near the phase transitions in ammonium halides
Yurtseven, Hasan Hamit (Elsevier BV, 2008-12-01)
This study concentrates on the temperature dependence of the Raman intensities for the lattice modes in ammonium halides (NH4Cl and NH4Br) close to phase transitions, We predict their intensities using the results of a shell model for the Raman polarizability within the framework of an Ising pseudospin-phonon coupled model.
Optimization of microwave-assisted extraction of phenolic compounds from tomato: Characterization by FTIR and HPLC and comparison with conventional solvent extraction
Baltacıoğlu, Hande; Baltacıoğlu, Cem; Okur, İlhami; Tanrıvermiş, Arif; Yalıç, Muharrem (Elsevier BV, 2021-03-01)
© 2021 Elsevier B.V.In the extraction of phenolic compounds from tomato, Microwave-Assisted Extraction (MAE) was used as a novel technology in this study and compared to conventional solvent extraction (CSE). The optimal extraction conditions for tomato were determined using the multi-level factorial design. For this purpose, different powers (360, 600 and 900 W) and times (30, 60 and 90 s) were used for MAE and also different temperatures (40, 50 and 60 °C) and times (10, 20 and 30 min) were used for CSE. ...
Evaluation of the radiative recombination mechanism in Si nanocrystals embedded in silica matrix
Righini, Marcofabio; Gnoli, Andrea; Razzari, Luca; Serincan, Ugur; Turan, Raşit (American Scientific Publishers, 2008-02-01)
We report measurements of the temperature dependence of photoluminescence (PQ life-time and efficiency of Si nanocrystals (Si-Nc) embedded in silica matrix. We use a practical technique based on lock-in acquisition that allows us to simultaneously evaluate, at each emission-energy, intensity and decay-time of the detected signal. Samples are prepared by Silicon-ion implantation in a SiO2 layer followed by thermal annealing. The implantation dose of Si ions ranges between 2 x 10(16) cm(-2) and 2 x 10(17) cm(...
Citation Formats
Ö. Ateş, “Design and construction of a sampling system that can collect PM10, PM2.5 and PM1 samples simultaneously from atmosphere,” Thesis (M.S.) -- Graduate School of Natural and Applied Sciences. Environmental Engineering., Middle East Technical University, 2019.