Introduction of solid-phase microextraction as a high-throughput sample preparation tool in laboratory analysis of prohibited substances.

Date

2014-05-25

Author

Boyacı, Ezel
Rodríguez-lafuente, Angel
Bojko, Barbara
Pawliszyn, Janusz

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https://hdl.handle.net/11511/76476

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Introduction of solid-phase microextraction as a high-throughput sample preparation tool in laboratory analysis of prohibited substances Boyacı, Ezel; Rodriguez-Lafuente, Angel; Bojko, Barbara; Pawliszyn, Janusz (Elsevier BV, 2014-01-27) A fully automated, high-throughput method based on thin-film solid-phase microextraction (SPME) and liquid chromatography-mass spectrometry was developed for simultaneous quantitative analysis of 110 doping compounds, selected from ten classes and varying in physical and chemical properties. Among four tested extraction phases, C18 blades were chosen, as they provided optimum recoveries and the lowest carryover effect. The SPME method was optimized in terms of extraction pH, ionic strength of the sample, wa...
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Citation Formats

E. Boyacı, A. Rodríguez-lafuente, B. Bojko, and J. Pawliszyn, “Introduction of solid-phase microextraction as a high-throughput sample preparation tool in laboratory analysis of prohibited substances.,” 2014, Accessed: 00, 2021. [Online]. Available: https://hdl.handle.net/11511/76476.