Protonation behaviour of some azaindoles and PKA determination of 3-hydroxy and 3-methoxy pyrazole derivatives.

Date

1974

Author

Gökçe, Bülent

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https://hdl.handle.net/11511/7991

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Graduate School of Natural and Applied Sciences, Thesis

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Protonation of acyl anion equivalents generated from acylphosphonates: nonhydride access to the aldehyde oxidation state from the carboxylic acid oxidation state Demir, Ayhan Sıtkı; Reis, Omer; Esiringu, Ilker; Reis, Barbaros; Baris, Sehriban (Elsevier BV, 2007-01-01) Acylphosphonates, which are easily available from carboxylic acids, are potent acyl anion precursors and undergo cyanide ion promoted phosphonate-phosphate rearrangement to provide the corresponding acyl anion equivalents as reactive intermediates. The protonation of these acyl anion equivalents furnished cyanohydrin O-phosphates in good yields. For the high yield formation of cyanohydrin O-phosphates from arylphosphonates THF should be used and from alkylphosphonates DME was used.
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Citation Formats

B. Gökçe, “Protonation behaviour of some azaindoles and PKA determination of 3-hydroxy and 3-methoxy pyrazole derivatives.,” Middle East Technical University, 1974.