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Stibine preconcentration in a quartz trap with subsequent atomization in the quartz multiatomizer for atomic absorption spectrometry
Date
2004-02-01
Author
Korkmaz, D
Dedina, J
Ataman, Osman Yavuz
Metadata
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This work is licensed under a
Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License
.
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A preliminary evaluation of a simple (bare) quartz tube trap for collection of SbH3 and for volatilization of trapped analyte with subsequent atomization in a multiple microflame quartz tube atomizer (multiatomizer) for atomic absorption spectrometry is presented. The influence of relevant experimental parameters on the collection/volatilization efficiency was investigated. The parameters studied Were: collection temperature and time, volatilization temperature and flow rates of air and hydrogen for the volatilization. Under optimized conditions, the collection/volatilization efficiency was 65%. For the collection time of 120 s (sample volume of 8 ml), the detection limit was 3.9 pg ml(-1), and the analytical plot was linear up to 1.25 ng ml(-1). Possible ways of improving the performance of the set-up as well as the collection/volatilization efficiency are suggested.
Subject Keywords
Sb
,
AAS
,
Coil
,
Elements
,
Selenium
,
Tube
,
Multiple microflame
,
Graphite-furnace
,
Hydride generation
,
Nickel tetracarbonyl generation
URI
https://hdl.handle.net/11511/31095
Journal
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY
DOI
https://doi.org/10.1039/b308883a
Collections
Graduate School of Natural and Applied Sciences, Article