Show/Hide Menu
Hide/Show Apps
Logout
Türkçe
Türkçe
Search
Search
Login
Login
OpenMETU
OpenMETU
About
About
Open Science Policy
Open Science Policy
Open Access Guideline
Open Access Guideline
Postgraduate Thesis Guideline
Postgraduate Thesis Guideline
Communities & Collections
Communities & Collections
Help
Help
Frequently Asked Questions
Frequently Asked Questions
Guides
Guides
Thesis submission
Thesis submission
MS without thesis term project submission
MS without thesis term project submission
Publication submission with DOI
Publication submission with DOI
Publication submission
Publication submission
Supporting Information
Supporting Information
General Information
General Information
Copyright, Embargo and License
Copyright, Embargo and License
Contact us
Contact us
Production and properties of phase separated porous glass
Date
2020-03-01
Author
Ertus, E. Burak
Vakifahmetoglu, Cekdar
Öztürk, Abdullah
Metadata
Show full item record
This work is licensed under a
Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License
.
Item Usage Stats
204
views
0
downloads
Cite This
A sodium borosilicate glass (SBG) was produced by conventional melt-quenching. As cast glass was heat treated to induce phase separation (SBG-HT), followed by acid leaching with HCl to dissolve one of the separated phases; i.e. alkali rich borate phase, so that a porous glass (PG) was obtained. In order to alter the pore structure, produced PG was subsequently alkali (NaOH) leached or alternatively heat treated. The samples were characterized by techniques including XRD, SEM, N-2 adsorption/desorption. The total pore volume for PG was found to be 0.314 cm(3)/g, reached to 0.370 cm(3)/g by alkali leaching, instead decreased to 0.227 cm(3)/g by heat treatment. The microhardness and tribological properties of SBG-HT and all PGs were evaluated by Vickers hardness and by pin on disk tribometer. For all PGs the microhardness values were lower, instead the wear rates were higher than that of the parent SBG-HT.
Subject Keywords
Process Chemistry and Technology
,
Materials Chemistry
,
Electronic, Optical and Magnetic Materials
,
Surfaces, Coatings and Films
,
Ceramics and Composites
URI
https://hdl.handle.net/11511/36000
Journal
CERAMICS INTERNATIONAL
DOI
https://doi.org/10.1016/j.ceramint.2019.10.232
Collections
Department of Metallurgical and Materials Engineering, Article
Suggestions
OpenMETU
Core
Fabrication of microporous ceramics from ceramic powders of quartz-natural zeolite mixtures
San, O; Abali, S; Hoşten, Çetin (Elsevier BV, 2003-01-01)
The possibility of producing ceramic powders suitable for the fabrication of microporous filters was investigated through the thermal treatment of the powder mixtures of a high-purity (99.09% SiO2) quartz and clinoptilolite type of natural zeolite. The quartz and zeolite, mixed in the ratio of 3:1 by weight, was wet ground in a ball mill, the powder was sieved on a 90-mum screen, and the undersize was dried and sintered in the powder form at the temperatures of 1000, 1100 and 1200degreesC for 7 h in an air ...
Fabrication and characterization of porous tricalcium phosphate ceramics
Koc, N; Timucin, M; Korkusuz, Feza (Elsevier BV, 2004-01-01)
Preforms of beta tricalcium phosphate (beta-TCP) ceramics were produced by using a modified slip casting technique. The slip was prepared by suspending custom-made TCP powder and PMMA beads in an aqueous medium stabilized with an acrylic deflocculant. Porous TCP ceramics were obtained by sintering the polymer-free preforms for 2 h at 1000 degreesC. The XRD pattern for the TCP ceramic indicated that the product was essentially pure beta-TCP. SEM examination of pore size and pore size distribution revealed th...
Morphology and magnetic properties of barium hexaferrite ceramics synthesized in x wt% NaCl-(100-x) wt% KCL molten salts
Aydogan, Eda; Kaya, Serap; Dericioğlu, Arcan Fehmi (Elsevier BV, 2014-01-01)
Micron size barium hexaferrite (BaFe12O19) platelets were prepared by the molten-salt synthesis method in various weight proportions of NaCl-KCl salt mixtures as a liquid medium. The effect of molten salt composition-x wt% NaCl and (100-x) wt% KCl-on the amount of barium hexaferrite phase formation, as well as, on the morphology and magnetic properties of the final products are discussed. Inductively coupled plasma-mass spectroscopy (ICP-MS) was used to determine the solubility of the starting materials in ...
Production and properties of tooth-colored yttria stabilized zirconia ceramics for dental applications
Kaplan, Melis; PARK, JONGEE; Kim, Soo Young; Öztürk, Abdullah (Elsevier BV, 2018-02-01)
Dense zirconia stabilized with 3 mol% yttria ceramics were produced in disc shape by first cold isostatically pressing at 100 MPa and then sintering at 1450 degrees C at ambient laboratory conditions. Coloring was accomplished by immersion the discs in NiCl2, MoCl3, and NiCl2 + MoCl3 solutions for 5, 30, and 60 s. Different concentrations (0.1, 0.25, and 0.5 wt%) were applied to get the color of natural tooth. The density, color, microhardness, fracture toughness, compressive strength, and wear rate of the ...
Production and characterization of hierarchically porous transparent glasses
Ertuş, Emre Burak; Öztürk, Abdullah; Department of Metallurgical and Materials Engineering (2020)
A sodium borosilicate glass (SBG) with nominal composition of 55.7SiO2-33.6B2O3-9.2Na2O-1.5Al2O3 (wt %) was produced by the conventional melt-quenching method. The as cast SBG was heat treated at various temperatures to induce phase separation. The phase separated glass was then acid (HCl) leached using three different HCl molarities to dissolve alkali-borate phase hence, to obtain a porous glass (PG). In order to control the pore structure and to find out a correlation between the pore architecture and the...
Citation Formats
IEEE
ACM
APA
CHICAGO
MLA
BibTeX
E. B. Ertus, C. Vakifahmetoglu, and A. Öztürk, “Production and properties of phase separated porous glass,”
CERAMICS INTERNATIONAL
, pp. 4947–4951, 2020, Accessed: 00, 2020. [Online]. Available: https://hdl.handle.net/11511/36000.