The synthesis and characterization of new metal-free and metallo phthalocyanines substituted with four dithiatetraoxa macrocyclic moieties

Date

2007-01-01

Author

Kantekin, Halit
Rakap, Murat
Misir, Mirac Nedim
Goek, Halil Zeki
Acar, Irfan

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New metal-free phthalocyanine ( 7) fused symmetrically in peripheral positions with four dithiatetraoxa macrocycles, has been synthesized by cyclotetramerization of the isoindoline-diimine derivative of macrocyclic 6. Metallophthalocyanine ( 8) was synthesized by reaction of phthalonitrile derivative ( 5) with anhydrous nickel( II) chloride. The new compounds were characterized by elemental analysis, H-1 and C-13-NMR, IR UV-Vis and mass spectroscopies.

Subject Keywords

Physical and Theoretical Chemistry, Materials Chemistry

URI

https://hdl.handle.net/11511/68134

Journal

JOURNAL OF COORDINATION CHEMISTRY

DOI

https://doi.org/10.1080/00958970701217412

Collections

Department of Chemistry, Article

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Citation Formats

H. Kantekin, M. Rakap, M. N. Misir, H. Z. Goek, and I. Acar, “The synthesis and characterization of new metal-free and metallo phthalocyanines substituted with four dithiatetraoxa macrocyclic moieties,” JOURNAL OF COORDINATION CHEMISTRY, pp. 1965–1972, 2007, Accessed: 00, 2020. [Online]. Available: https://hdl.handle.net/11511/68134.