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One-pot synthesis of functionalized 1,4-thiazepine derivatives from N-(2,4-pentadiynyl)-beta-enaminones
Date
2018-08-23
Author
Yılmaz, Elif Serel
Zora, Metin
Metadata
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URI
https://hdl.handle.net/11511/75514
Conference Name
256th National Meeting and Exposition of the American-Chemical-Society (ACS) - Nanoscience, Nanotechnology and Beyond, (AUG 19-23, 2018)
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Department of Chemistry, Conference / Seminar
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One-pot synthesis of functionalized 1,4-thiazepine derivatives from N-(2,4-pentadiynyl)-beta-enaminones
Ertem Yılmaz, Elif; Zora, Metin (2018-08-19)
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We describe the preliminary results of one-pot syntheses of various N-substituted 2-methyl-4,5,6,7-tetrahydroindole derivatives from 2-(2-bromoailyl)cyclohexanone and the corresponding primary amines in good yields. Aliphatic amines were directly converted to tetrahydroindoles, whereas aromatic amines needed an extra base treatment step to complete the transformation.
One-Pot Synthesis of 2-Acetyl-1 H-pyrroles from N-Propargylic β-Enaminones via Intermediacy of 1,4-Oxazepines
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A one-pot two-step protocol for the synthesis of 2-acetyl-1H-pyrroles from N-propargylic β-enaminones was described. When treated with zinc chloride in refluxing chloroform, N-propargylic β-enaminones produced in situ 2-methylene-2,3-dihydro-1,4-oxazepines, which, upon further refluxing in methanol with zinc chloride, afforded 2-acetyl-1H-pyrroles. The process was found to be general for a wide variety of N-propargylic β-enaminones and yielded a diverse range of 2-acetyl-1H-pyrroles in good to high yields w...
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E. S. Yılmaz and M. Zora, “One-pot synthesis of functionalized 1,4-thiazepine derivatives from N-(2,4-pentadiynyl)-beta-enaminones,” Boston, MA, 2018, vol. 256, Accessed: 00, 2021. [Online]. Available: https://hdl.handle.net/11511/75514.