Determination of selenium in human diet by Zeeman effect graphite furnace AAS

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1988
Arı, Ülkü

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The selenium content of Turkish diets was determined by Zeeman effect graphite furnace atomic absorption spectrometry (GFAAS). Samples, collected from two different socioeconomic groups by duplicate portion technique, were digested with concentrated nitric acid in acid bombs, and hydrogen peroxide was added for complete oxidation. The digested solutions were then analyzed by GFAAS with the nickel chemical modifier addition. The detection limit for Se(VI) was 10.5 ng/mL for aqueous standard solutions. Averag...
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A post-irradiation radiochemical separation technique was tested for the determination of selenium levels in diet samples, collected by using a duplicate portion technique, from both rural and urban population groups in Turkey. The technique involved sample irradiation, acid digestion, selective distillation, precipitation and filtration steps. During the separations it was possible to determine the yield of each sample using a stable selenium carrier. An average chemical yield of 71 +/- 3% was obtained ...
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ThephytatecontentofdailydietsamplesfromuppermiddleclassfamiliesinTurkeywasdeter-minedbyphosphorus-31Fouriertransformnuclearmagneticresonancespectroscopy(31PFTNMR).Samples,collectedbyaduplicate-portiontechnique,werehomogenizedandfreeze-dried.Dietsam-pleswerestirredfor0.5hinaqueous3%(w/v)trichloroaceticacid,EDTAwasadded,andthepHwasadjustedto4.5±0.5beforeanalysis.Theaveragephytatecontentof10dietsampleswasfoundtobe1.55±0.70g/kg
Citation Formats
Ü. Arı, “Determination of selenium in human diet by Zeeman effect graphite furnace AAS,” Middle East Technical University, 1988.