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Microwave initiated polymerization of trihalophenyleneoxide and aniline
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Date
2011
Author
Levent, Fulya
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The aim of the study is to synthesize poly(dibromophenyleneoxide) and polyaniline separately applying different microwave energies (90-900 watt), water amounts (1-5 ml) and time intervals (2-10 min) and investigate the effects of these parameters on the percent conversion of the polymers. The synthesis of poly(dibromophenyleneoxide) (P), radical ion polymer (RIP) and crosslinked polymer (CLP) were achieved by using tribromophenol (TBP) and Ca(OH)2 via microwave energy in a very short time interval. P and RIP were characterized by ATR-FTIR, 1H-NMR, 13C-NMR, TGA-FTIR, ESR, GPC, UV-VIS, DLS and SEM. Crosslinked polymers were characterized by ATR-FTIR and TGA-FTIR and polyaniline was characterized by ATR-FTIR.
Subject Keywords
Polymers.
,
Polymerization.
URI
http://etd.lib.metu.edu.tr/upload/12612941/index.pdf
https://hdl.handle.net/11511/20458
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Graduate School of Natural and Applied Sciences, Thesis
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F. Levent, “Microwave initiated polymerization of trihalophenyleneoxide and aniline,” M.S. - Master of Science, Middle East Technical University, 2011.
