Synthesis and characterization of poly(Phenylene oxide)s through various nickel(II) complexes in solution

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1998
Karabey, Leyla
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https://hdl.handle.net/11511/2164
Graduate School of Natural and Applied Sciences, Thesis

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SYNTHESIS AND CHARACTERIZATION OF POLY(DICHLOROPHENYLENE OXIDE)S THROUGH SOLID-STATE THERMAL-DECOMPOSITION OF BIS(PYRIDINE)BIS(TRICHLOROPHENOXO)COPPER(II) COMPLEXES
BASTURKMEN, M; KISAKUREK, D (Elsevier BV, 1993-01-01)
Thermal polymerization of bis(pyridine)bis(trichlorophenoxo)copper(II) was achieved in the solid state for the first time. The time and temperature effect on polymer molecular weight, percentage yield and the structure of polymer was first studied, at constant temperature and then for constant decomposition time. Polymers were characterized by i.r., H-1 n.m.r. and C-13 n.m.r. The molecular weights of the polymers were obtained by viscometric measurements at 30-degrees-C in toluene and glass transition tempe...
SYNTHESIS AND CHARACTERIZATION OF POLY(DICHLOROPHENYLENE OXIDE)S BASED ON THE ELECTROOXIDATION OF BIS(2,4,6-TRICHLOROPHENOXO)BIS(PYRIDINE)COPPER(II) COMPLEX
SEN, S; KISAKUREK, D (Elsevier BV, 1993-01-01)
Electroinitiated polymerization of bis(2,4,6-trichlorophenoxo)bis(pyridine)copper(II) complex was achieved in dimethylformamide by constant potential electrolysis under air and N2. The polymers obtained at several potentials were characterized by H-1 n.m.r., C-13 n.m.r., FTi.r. and d.s.c., and were found to be branched. The kinetics of the polymerization were followed by in situ cyclic voltammetry measurements at 13.5 and 20-degrees-C during electrolysis. As found for the thermal polymerization of this comp...
Synthesis and characterization of poly(dihalophenylene oxide)s through solid state thermal decomposition of cerium(IV) complexes of trihalogenated phenols
Şentürk, Özlem; Kısakürek, Duygu; Department of Chemistry (2000)
Synthesis and characterization of poly(dihalophenylene oxide)s through bis(trihalophenolato) (ethylene-diamine)(pyridine)nickel(II) complexes in solution in the presence of iodine
Molu, LK; Kisakurek, D (2001-10-17)
Synthesis and characterization of poly(dibromophenylene oxide)s through thermal decomposition of various transition metal complexes in solid state.
Şanlı, Pınar; Kısakürek, Duygu; Aras, Leyla; Department of Chemistry (2002)
In this study, synthesis and characterization of poly(dibromophenylene oxide)s though thermal decomposition of bis(2,4,6-tribromophenolato)di(N- methyl imidazole) Cu(II), bis(2,4,6-tribromophenolato)di(N-methyl illimidazole)Co(II) and bis(2,4,6-tribromophenolato)di(N-methyl imidazole)Ni(II) complexes in solid state was examined. For the characterization of complexes FTIR, DSC, mass spectroscopy, magnetic susceptibility and C, H,N elemental analysis were performed. Syntheses of the polymer were achieved by t...
Citation Formats
L. Karabey, “Synthesis and characterization of poly(Phenylene oxide)s through various nickel(II) complexes in solution,” Middle East Technical University, 1998.
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