Flow injection-hydride generation-infrared spectrophotometric determination of Pb

Date

2005-04-30

Author

Cankur, O
Korkmaz, D
Ataman, Osman Yavuz

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novel analytical technique has been suggested for determination of Pb usingformation of PbH4(g) by chemical reduction and its subsequent spectrophotometric measurement in IR region, using the peak at 1821.4 cm(-1). The range of measurements is 1.0-30.0 mg l(-1) using a sample of 1.0 ml in flow injection mode. The 3 sigma limit of detection is 0.28 mg l(-1). The method has been applied to standard reference materials of Waste Water, EU-L-1, lead-base bearing metal 53e and Soil/Sediment #4 as well as soil samples collected from heavy traffic areas in Ankara.

Subject Keywords

pb, Hydride generation, Molecular absorption, Dispersive infrared, FTIR, Soil

URI

https://hdl.handle.net/11511/30174

Journal

TALANTA

DOI

https://doi.org/10.1016/j.talanta.2004.12.034

Collections

Graduate School of Natural and Applied Sciences, Article

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Citation Formats

O. Cankur, D. Korkmaz, and O. Y. Ataman, “Flow injection-hydride generation-infrared spectrophotometric determination of Pb,” TALANTA, pp. 789–793, 2005, Accessed: 00, 2020. [Online]. Available: https://hdl.handle.net/11511/30174.