Preparation of lead zirconate titanate (Pb(Zr0.52Ti0.48)O-3) by homogeneous precipitation and calcination

1998-05-06
Oren, EE
Tas, AC
Aqueous solutions of lead chloride (PbCl2), zirconium oxychloride (ZrOCl2.8H(2)O) and titanium tetrachloride (TiCl4), in appropriate volumetric amounts, were used as the starting materials in the synthesis of phase-pure Pb(Zr0.52Ti0.48)O-3 powders. Preparation of the phase-pure PZT powders were achieved, in the presence of urea (CH4N2O), by the chemical powder synthesis route of homogeneous precipitation.

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Preparation of lead zirconate titanate (Pb(Zr0.52Ti0.48)O-3) by homogeneous precipitation and calcination
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Preparation of phase-pure PZT (Pb(Zr0.52Ti0.48)O-3) powders was achieved, in the presence of urea (CH4N2O), by homogeneous precipitation. Aqueous solutions of PbCl2, ZrOCl2. 8H(2)O, and TiCl4 were used as the starting materials in the synthesis of phase-pure PZT powders. Phase evolution behavior of precursor powders was studied by powder X-ray diffraction (XRD) in air, over the temperature range of 90 degrees to 750 degrees C. The morphology of the formed powders was studied by scanning electron microscopy ...
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Citation Formats
E. Oren and A. Tas, “Preparation of lead zirconate titanate (Pb(Zr0.52Ti0.48)O-3) by homogeneous precipitation and calcination,” 1998, vol. 100, p. 105, Accessed: 00, 2020. [Online]. Available: https://hdl.handle.net/11511/64596.