Show/Hide Menu
Hide/Show Apps
Logout
Türkçe
Türkçe
Search
Search
Login
Login
OpenMETU
OpenMETU
About
About
Open Science Policy
Open Science Policy
Open Access Guideline
Open Access Guideline
Postgraduate Thesis Guideline
Postgraduate Thesis Guideline
Communities & Collections
Communities & Collections
Help
Help
Frequently Asked Questions
Frequently Asked Questions
Guides
Guides
Thesis submission
Thesis submission
MS without thesis term project submission
MS without thesis term project submission
Publication submission with DOI
Publication submission with DOI
Publication submission
Publication submission
Supporting Information
Supporting Information
General Information
General Information
Copyright, Embargo and License
Copyright, Embargo and License
Contact us
Contact us
Synthesis and Characterization of Surface Modified Fullerene
Date
2012-01-01
Author
Kanbur, Yasin
Kucukyavuz, Zuhal
Metadata
Show full item record
This work is licensed under a
Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License
.
Item Usage Stats
182
views
0
downloads
Cite This
Fullerenes were chemically functionalized by using sulphuric acid and nitric acid. The functionalization was done with two different acid ratio. The functionalized nanotubes were characterized with Fourier transform infrared spectroscopy and X-ray photonelectron spectroscopy (XPS), elemental analysis, scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Sulfonation of fullerene increased the electrical conductivity of fullerenes up to 0.027 S/cm. TEM micrographs showed that sulfonation improves the dispersion of fullerene in water. Zeta potential measurements also proved this result.
Subject Keywords
Fullerene
,
Electrical conductivity
,
Surface modification
,
Zeta potential
URI
https://hdl.handle.net/11511/65583
Journal
FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES
DOI
https://doi.org/10.1080/1536383x.2010.533306
Collections
Department of Chemistry, Article
Suggestions
OpenMETU
Core
Preparation and characterization of ni-nitrilotriacetic acid bearing Poly(Methacrylic acid) coated superparamagnetic magnetite nanoparticles
TURAL, Bilsen; KAYA, Murat; Özkan, Necati; Volkan, Mürvet (2008-02-01)
Stable superparamagnetic magnetite (Fe3O4) nanoparticles were synthesized via co-precipitation in the presence of poly(methacrylic acid) (PMAA) in aqueous solution. The polymer coated Fe3O4 nanoparticles were characterized using transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction, thermal analysis, and vibrating sample magnetometry (VSM) techniques. These measurements reveal the presence of magnetite nanoparticles with a size of approximately 8 nm inside...
Synthesis and characterization of thiophen-3-yl acetic acid 4-pyrrol-1-yl phenyl ester and its conducting polymers
BINGÖL, Bahar; GÜNER, Yusuf; Çırpan, Ali; Toppare, Levent Kamil (Informa UK Limited, 2005-08-01)
Thiophen-3-yl acetic acid 4-pyrrol-1-yl phenyl ester (TAPE) monomer was synthesized via reaction of thiophen-3-yl acetyl chloride with 4-pyrrol-1-yl phenol. Homopolymers were achieved by using electrochemical and chemical polymerization techniques. Copolymers of TAPE with bithiophene or pyrrole were synthesized by potentiostatic electrochemical polymerization in acetonitrile-tetrabutylammonium tetrafluoroborate (TBAFB) solvent-electrolyte couple. The chemical structures were confirmed by both Nuclear Magnet...
Synthesis and characterization of thiophen-3-yl-acetic acid 4-pyrrol-1-yl-phenyl ester and its conducting polymers
Bingöl, Bahar; Toppare, Levent Kamil; Department of Chemistry (2003)
Thiophen-3-yl acetic acid 4-pyrrol-1-yl phenyl ester (TAPE) monomer was synthesized by the reaction of thiophene acetic acid with thionyl chloride, and further reaction of thiophen-3-yl-acetyl chloride with 4-pyrrol-1-yl phenol. Electrochemical behavior of this monomer (TAPE) was determined by cyclic voltammetry. Homopolymers were achieved both by using electrochemical and chemical polymerization techniques. Copolymers of TAPE in the presence of bithiophene and pyrrole were synthesized by potentiostatic ele...
Synthesis, characterization, and electrochromic properties of conducting poly(hexanedioic acid bis-(2-thiophen-3-yl-ethyl ester) and its copolymer with thiophene
CAMURLU, P; Çırpan, Ali; Toppare, Levent Kamil (Elsevier BV, 2004-10-14)
Hexanedioic acid bis-(2-thiophen-3-yl-ethyl) ester (HABTE) was synthesized via the reaction of 3-thiophene ethanol with adipoyl chloride. Resulting monomer was electrochemically homopolymerized in the presence of tetrabutylammonium tetrafluoroborate as the supporting electrolyte, in acetonitrile/borontrifloride ethylether solvent mixture (8:2, v/v). Copolymerization in the presence of thiophene was achieved in TBAFB/AN. Resulting homo and copolymers were characterized via CV, FTIR, DSC, TGA, SEM, and UV-vis...
Surface Modification and Characterization of Multi-Walled Carbon Nanotube
Kanbur, Yasin; Kucukyavuz, Zuhal (Informa UK Limited, 2011-01-01)
Multi-walled carbon nanotubes (MWCNTs) were chemically functionalized by using sulfuric acid and nitric acid. The functionalization was done with two different acid ratio. The functionalized nanotubes were characterized with Fourier Transform Infrared Spectroscopy, X-Ray Photon Spectroscopy, Thermal Gravimetric Analysis, Elemental Analysis, Scanning Electron Microscopy (SEM), and Transmission Electron Microscopy. Sulfonation of carbon nanotubes (CN) increased the electrical conductivity of carbon nanotubes ...
Citation Formats
IEEE
ACM
APA
CHICAGO
MLA
BibTeX
Y. Kanbur and Z. Kucukyavuz, “Synthesis and Characterization of Surface Modified Fullerene,”
FULLERENES NANOTUBES AND CARBON NANOSTRUCTURES
, pp. 119–126, 2012, Accessed: 00, 2020. [Online]. Available: https://hdl.handle.net/11511/65583.