Trimethyl 4,4′,4′′-(ethene-1,1,2-triyl)tribenzoate

2020-03-01
Lesley, Melvin J
ÖZHAN, KORAY
Sung, Herman H-Y
Williams, Ian D
The title compound, C26H22O6, is formed as the major product from the reaction between syn-1,2-bis­(pinacolatoboron)-1,2-bis­(4-methyl­carb­oxy­phen­yl)ethene and excess methyl 4-iodo­benzoate in basic DMSO using a palladium catalyst at 80°C via Suzuki coupling followed by protodeboronation. Crystals were grown by slow evaporation of a hexa­nes solution at room temperature.
Citation Formats
M. J. Lesley, K. ÖZHAN, H. H.-Y. Sung, and I. D. Williams, “Trimethyl 4,4′,4′′-(ethene-1,1,2-triyl)tribenzoate,” IUCrData, vol. 5, no. 3, pp. 0–0, 2020, Accessed: 00, 2021. [Online]. Available: http://scripts.iucr.org/cgi-bin/paper?S2414314620004174.