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Synthesis and characterization of poly(dihalophenylene oxide)s by using thermal decomposition of Ce(IV) complexes in solid state.
Date
2001
Author
Çelik, Güler
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https://hdl.handle.net/11511/11538
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Graduate School of Natural and Applied Sciences, Thesis
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In this study, synthesis and characterization of poly(dibromophenylene oxide)s though thermal decomposition of bis(2,4,6-tribromophenolato)di(N- methyl imidazole) Cu(II), bis(2,4,6-tribromophenolato)di(N-methyl illimidazole)Co(II) and bis(2,4,6-tribromophenolato)di(N-methyl imidazole)Ni(II) complexes in solid state was examined. For the characterization of complexes FTIR, DSC, mass spectroscopy, magnetic susceptibility and C, H,N elemental analysis were performed. Syntheses of the polymer were achieved by t...
SYNTHESIS AND CHARACTERIZATION OF POLY(DICHLOROPHENYLENE OXIDE)S THROUGH SOLID-STATE THERMAL-DECOMPOSITION OF BIS(PYRIDINE)BIS(TRICHLOROPHENOXO)COPPER(II) COMPLEXES
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Thermal polymerization of bis(pyridine)bis(trichlorophenoxo)copper(II) was achieved in the solid state for the first time. The time and temperature effect on polymer molecular weight, percentage yield and the structure of polymer was first studied, at constant temperature and then for constant decomposition time. Polymers were characterized by i.r., H-1 n.m.r. and C-13 n.m.r. The molecular weights of the polymers were obtained by viscometric measurements at 30-degrees-C in toluene and glass transition tempe...
Synthesis and characterization of poly (dichlorophenylene oxides) through solid state thermal decomposition of bis(pyridine) bis(trichlorophenoxo) copper (II) and bis (pyridine) bis (trichlorophenoxo) Cobalt(II) complexes
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G. Çelik, “Synthesis and characterization of poly(dihalophenylene oxide)s by using thermal decomposition of Ce(IV) complexes in solid state.,” Middle East Technical University, 2001.