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Synthesis and characterization of poly(dihalophenylene oxides) from the decomposition of bis(pyridine)bis(trihalophenoxo) copper (II) complexes
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007334.pdf
Date
1989
Author
Şen, Şadi
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Subject Keywords
Polymers and polymerization.
,
Electrolysis.
,
Electrochemistry.
,
Copper.
,
Phenols.
,
Pyridine.
URI
https://hdl.handle.net/11511/11646
Collections
Graduate School of Natural and Applied Sciences, Thesis
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SYNTHESIS AND CHARACTERIZATION OF POLY(DICHLOROPHENYLENE OXIDE)S BASED ON THE ELECTROOXIDATION OF BIS(2,4,6-TRICHLOROPHENOXO)BIS(PYRIDINE)COPPER(II) COMPLEX
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Electroinitiated polymerization of bis(2,4,6-trichlorophenoxo)bis(pyridine)copper(II) complex was achieved in dimethylformamide by constant potential electrolysis under air and N2. The polymers obtained at several potentials were characterized by H-1 n.m.r., C-13 n.m.r., FTi.r. and d.s.c., and were found to be branched. The kinetics of the polymerization were followed by in situ cyclic voltammetry measurements at 13.5 and 20-degrees-C during electrolysis. As found for the thermal polymerization of this comp...
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Ş. Şen, “Synthesis and characterization of poly(dihalophenylene oxides) from the decomposition of bis(pyridine)bis(trihalophenoxo) copper (II) complexes,” Ph.D. - Doctoral Program, Middle East Technical University, 1989.