Electrochemical reduction of molybdenium compounds to form molybdenium powder

Akpınar, Bengisu
Erdoğan, Metehan
Karakaya, İshak


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The production of tungsten by direct current reduction has been investigated. Experimental studies involved the electrochemical reduction of the solid tungsten compounds tungsten trioxide (WO(3)) and calcium tungstate (CaWO(4)) in the form of an assembled cathode of porous pellets attached to a current collector. Molten calcium chloride and a molten solution of calcium chloride and sodium chloride at eutectic composition, 48 pct mol NaCl, were used as the electrolytes. Reduced samples were characterized by ...
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A new monomer, 4-(thiophen-3-yl methyleneamino)benzene sulfonate) (ThSA), was synthesized and characterized. Electrochemical polymerization of ThSA yields a water-soluble and self-doped polymer (PThSA). This polymer was characterized by FT-IR, NMR, DSC, XRD and conductivity measurements. (C) Koninklijke Brill NV, Leiden, 2008
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The Al-Sc alloy formation by the reduction of Sc containing compounds in a molten salt containing CaCl2 was investigated in this study. The preliminary tests revealed that Al3Sc intermetallic, which gives the superior properties to this alloy, was successfully formed and distributed homogeneously throughout the Al matrix. XRD, SEM-EDS and optical microscopy analyses were used to confirm the results.
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Citation Formats
B. Akpınar, M. Erdoğan, and İ. Karakaya, “Electrochemical reduction of molybdenium compounds to form molybdenium powder,” presented at the 231 st ECS Meeting ( 29 Mayıs - 02 Haziran 2017), 2017, Accessed: 00, 2021. [Online]. Available: http://ma.ecsdl.org/content/MA2017-01/20/1105.abstract?sid=edf5f1aa-ddb2-4b22-82fa-a864e042697f.