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Influence of ultrasonically assisted synthesis on particle size of magnetic nanoparticles
Date
2013-10-01
Author
KÜÇÜK, Burcu
Özkan, Necati
Volkan, Mürvet
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Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License
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Poly(methacrylic acid)(PMAA) coated magnetite (Fe3O4) nanoparticles were synthesized via co-precipitation in aqueous solution with the use of conventional magnetic stirring and ultrasonic agitation. It has been shown that the ultrasonic agitation during the synthesis of magnetite particles decreased the size of PMAA-coated magnetic agglomerates significantly. The primary particle size of iron oxide particles was determined as approximately 10 nm by X-ray diffraction method (Scherer's equation). The volume weighted mean size (D [4,3]) of PMAA coated magnetite particles was determined as about 80 nm using laser diffraction technique.
Subject Keywords
Magnetic materials
URI
https://hdl.handle.net/11511/31586
Journal
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS
DOI
https://doi.org/10.1016/j.jpcs.2013.04.027
Collections
Graduate School of Natural and Applied Sciences, Article
Citation Formats
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BibTeX
B. KÜÇÜK, N. Özkan, and M. Volkan, “Influence of ultrasonically assisted synthesis on particle size of magnetic nanoparticles,”
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS
, vol. 74, no. 10, pp. 1426–1432, 2013, Accessed: 00, 2020. [Online]. Available: https://hdl.handle.net/11511/31586.